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Synthesis and Structure of 2-Hydroxy-2-methyl-1,3-bis-(methyl 3′,4′,6′-tri-O-acetyl-β-D-glucopyranosid-2-yl) -imidazolidine-4,5-dione (IV).

✍ Scribed by Andrzej Temeriusz; Magdalena Rowinska; Boguslawa Piekarska-Bartoszewicz; Romana Anulewicz-Ostrowska; Michal K. Cyranski


Publisher
John Wiley and Sons
Year
2006
Weight
17 KB
Volume
37
Category
Article
ISSN
0931-7597

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NMR study of methyl 3,4,6-tri-O-acetyl-2
✍ Iwona Wawer; Małgorzata Weychert; Jan Klimkiewicz; Bogusława Piekarska-Bartoszew 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 117 KB 👁 1 views

Five derivatives of methyl 3,4,6-triacetyl-2-deoxy-(3@-dialkylureido)-b-D-glucopyranoside were studied by 1H and 13C, NMR spectroscopy in solutions and by 13C NMR spectroscopy in the solid state. Sterically CDCl 3 crowded substituents such as n-hexyl and cylcohexyl change the chemical shifts of H-1,