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Synthesis and Structure Determination of the Disordered VV–P Compound (NH4)2VIVO(VV2−xPxO7)

✍ Scribed by C. Ninclaus; R. Retoux; D. Riou; G. Férey

Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
327 KB
Volume
122
Category
Article
ISSN
0022-4596

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Hydrothermal Synthesis and Crystal Structure of an Unusual Compound: [Cu(en)2]4[SiMo8VV4O40(VIVO)2][MoO4]2·5H2O
✍ Guoyou Luan; Yangguang Li; Enbo Wang; Zhengbo Han; Changwen Hu; Ninghai Hu; Heng 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 363 KB

has been hydrothermally synthesized and structurally characterized by single-crystal X-ray diffraction. Black crystals crystallize in the tetragonal system, space group I4/m, a = b = 14.019(2) A ˚, c = 20.341(4) A ˚, V =3997.9(11) A ˚3, Z = 2, k(MoKa) = 0.71073 A ˚(R(F) = 0.0443 for 1819 reflections