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Synthesis and structural characterization of K(MoO2)(PO4) · H2O, and its topotatic reaction to form KMoO2PO4

✍ Scribed by R. Peascoe; A. Clearfield


Publisher
Elsevier Science
Year
1991
Tongue
English
Weight
641 KB
Volume
95
Category
Article
ISSN
0022-4596

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Leucophosphite K[Fe2(PO4)2(OH)(H2O)]·H2O
✍ Stefan Dick; Thomas Zeiske 📂 Article 📅 1997 🏛 Elsevier Science 🌐 English ⚖ 337 KB

Hydrogen atom positions in leucophosphite K[Fe 2 (PO 4 ) 2 (OH)(H 2 O)] • H 2 O were elucidated by Rietveld refinement of a powder neutron scattering diffractogram. Crystal data: a ‫؍‬ 975.6(3), b ‫؍‬ 966.4(3), c ‫؍‬ 976.9(4) pm, ‫؍‬ 102.43(2)°°, R wp ‫؍‬ 0.084. This experiment proved that the Fe-at