C{ 1 H}-NMR (125.8 MHz, C 6 D 6 , RT): d 14.9 (SMe), 38.6 (CH 2 ), 127.4, 129.6, 130.8, 130.9, 136.1, 143.3 (arom. C); 29 Si-NMR (99.4 MHz, CD 2 Cl 2 , À 80 8C): d À 104.3 (t, 1 J(Si,P) 37,8 Hz); 29 Si-NMR (99.4 MHz, C 6 D 6 , RT): d À 67.8 ( 1 J(Si,H) 251, 1 J(P,Si) 19.8 Hz); 29 Si{ 1 H}-CP-MAS-NMR
Synthesis and Structural Characterization of Graphite-Like [(Me3Sn)3O]Cl
✍ Scribed by Bodo Räke; Peter Müller; Herbert W. Roesky; Isabel Usón
- Publisher
- John Wiley and Sons
- Year
- 1999
- Tongue
- English
- Weight
- 125 KB
- Volume
- 38
- Category
- Article
- ISSN
- 0044-8249
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📜 SIMILAR VOLUMES
can lead to oriented domains and/or antiphase boundaries. High resolution electron microscopic investigations will help us elucidate these features. Finally, numerous crystals exhibit both phenomena simultaneously (Fig. 5c); microtwins can then appear in only one of the crystal domains (domain 11).
The first selenite chloride hydrates, Co(HSeO 3 )-Cl ´3 H 2 O and Cu(HSeO 3 )Cl ´2 H 2 O, have been prepared from solution and characterised by single-crystal X-ray diffraction. The cobalt phase adopts an unusual ªone-dimensionalº structure built up from vertex-sharing pyramidal [HSeO 3 ] 2± , and o