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Synthesis and Structural Characterization of a Sterically Crowded Acylguanidinate: RFC(=O)N=C(NMe2)2 (RF: 2,4,6-Tris(trifluoromethyl)phenyl).

✍ Scribed by Zhaofu Fei; Axel K. Fischer; Frank T. Edelmann


Publisher
John Wiley and Sons
Year
2003
Weight
91 KB
Volume
34
Category
Article
ISSN
0931-7597

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Synthesis and Structural Characterizatio
✍ Srinivasan Natarajan; Anthony K. Cheetham πŸ“‚ Article πŸ“… 1998 πŸ› Elsevier Science 🌐 English βš– 478 KB

A new layered tin(II) phosphate [Sn 2 (PO 4 ) 2 ] 2؊ [C 2 N 2 H 10 ] 2Ψ‰ β€’ H 2 O was synthesized by hydrothermal technique. It crystallizes in monoclinic space group P2 1 /c (No. 14) with lattice parameters a ‫؍‬ 9.4112(1) A s ; b ‫؍‬ 8.5998(1) A s ; c ‫؍‬ 15.9921(2) A s ; ‫؍‬ 100.009(1)Β°; V ‫؍‬ 12