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Synthesis and Reactivity of α,α-Dichloroglycyl Peptides

✍ Scribed by Dr. Stefan Jaroch; Dipl.-Chem. Thomas Schwarz; Prof. Dr. Wolfgang Steglich; Dipl.-Chem. Peter Zistler

Publisher
John Wiley and Sons
Year
1993
Tongue
English
Weight
240 KB
Volume
32
Category
Article
ISSN
0044-8249

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✦ Synopsis

nBuLi solution (5 mmol: in hexanej added. On warming to room temperature the original yellow solution changed color from green to reddish-brown. and gdS evolution was observed. After the mixture had been stirred at room temperature for 30 min the resulting clear yellow solution was refrigerated overnight. This afforded very pale yellow crystals of 1 [first batch yield, 0.76 g.

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probably differentpolypeptide chains cannot yet be answered. Investigations of the amino acid sequence [5] also permit no definite conclusions so far.