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Synthesis and Reactivity of (CF3)2PN3, (CF3)2AsN3, CF3AsClN3 and CF3As(N3)2 Azides

✍ Scribed by H. G. Ang

Publisher: John Wiley and Sons
Year: 2004
Weight: 7 KB
Volume: 35
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200445275

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## Abstract The relative rate technique has been used to determine the rate constants of the reactions of OH radicals with CF~3~CClCCl~2~ (__k__~1~), CF~3~CClCClCF~3~ (__k__~2~) and CF~3~CFCFCF~3~ (__k__~3~). Experiments were carried out at (298±2) K and atmospheric pressure using ultrapure nitr

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Rate constant ratios, k d /k c , for the disproportionation/combination reaction at a temperature of 295 Ϯ 2 K, have been measured as 0.034 Ϯ 0.009 for the collision between CF 3 CH 2 CF 2 ϩ CF 3 radicals and as 0.075 Ϯ 0.019 for CF 3 CH 2 CF 2 ϩ CF 3 CH 2 CF 2 radicals. The effect of the two fluori