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Synthesis and reaction of 5,6,7,8-tetrahydro-4H-oxazolo[4,5-c]azepin-4-ones

✍ Scribed by Young Kook Koh; Ki-Hwan Bang; Hong-Seok Kim

Publisher
Journal of Heterocyclic Chemistry
Year
2001
Tongue
English
Weight
60 KB
Volume
38
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

The synthesis of 5,6,7,8‐tetrahydro‐4__H__‐oxazolo[4,5‐c]azepin‐4‐ones 5a,b and 1,3‐benzoxazol‐4‐amines 4a,b are described starting from 4,5,6,7‐tetrahydro‐1,3‐benzoxazol‐4‐ones. Thionation of 5a,b followed by alkylation with ethyl bromoacetate led to the corresponding S‐alkyl azepines 7a,b.

📜 SIMILAR VOLUMES

ChemInform Abstract: Synthesis and React
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