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Synthesis and properties of sym-triazine derivatives. 7. Synthesis of pyridyl-substituted 2-amino- and 2,4-diamino-sym-triazines

✍ Scribed by V. I. Kelarev; R. A. Karakhanov; M. Bellul'; R. L. Ushakova; A. I. Mikaya

Publisher: Springer US
Year: 1988
Tongue: English
Weight: 520 KB
Volume: 24
Category: Article
ISSN: 0009-3122
DOI: 10.1007/bf00755698

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g (2 mmole) of freshly distilled benzoyl chloride; the mixture was stirred for 4 h at ca. 20~ basified with NaOR solution, and extracted with chloroform. The extract was dried over magnesium sulfate. After solvent evaporation there was obtained 0.3 g (60%) of yellow crystals, mp 187-189~ (from a mi