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Synthesis and properties of p-dialkylbenzenes

✍ Scribed by A. D. Petrov; G. I. Nikishin; V. D. Vorob'ev


Book ID
112434894
Publisher
Springer
Year
1960
Tongue
English
Weight
474 KB
Volume
9
Category
Article
ISSN
1573-9171

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The 19F-NMR spectrum at 30 "C contains one very broad signal, which becomes narrower with decrease in the temperature. At -60Β°C the chemical shift amounts to -55.1 ppm referred to CC13F as internal standard. The mass spectrum of (3) contains the typical fragments SC-NCS ( m / e = 102), CNCS (70), SC