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Synthesis and Properties of O-β-D-ribofuranosyl-(1″→2′)-guanosine-5″- O-phosphate and Its Derivatives

✍ Scribed by Ekaterina V. Efimtseva; Alexandra A. Shelkunova; Sergey N. Mikhailov; Koen Nauwelaerts; Jef Rozenski; Eveline Lescrinier; Piet Herdewijn

Publisher
John Wiley and Sons
Year
2003
Tongue
German
Weight
172 KB
Volume
86
Category
Article
ISSN
0018-019X

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✦ Synopsis

Abstract

The efficient synthesis of O‐β‐D‐ribofuranosyl‐(1″→2′)‐guanosine‐5″‐O‐phosphate and O‐β‐D‐ribofuranosyl‐(1″→2′)‐adenosine‐5″‐O‐phosphate, minor tRNA components, have been developed, and their conformational properties were examined by NMR spectroscopy.

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## Abstract The dinucleoside phosphate __Π__~d~p__Π__~d~ (**4**) was synthesized from the monomers 1‐(5′‐__O__‐monomethoxytrityl ‐ 2′ ‐ deoxy ‐ β ‐ D ‐ ribofuranosyl) ‐ 2 (1 __H__) ‐ pyridone ((MeOTr) __Π__~d~, **2**) and 1‐(5′‐__O__‐phosphoryl‐3′‐__O__‐acetyl‐2′‐deoxy‐β‐D‐ribofuranosyl)‐(1__H__)‐p