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Synthesis and Optical Resolution of Aminophosphines with Axially Chiral C(aryl)−N(amine) Bonds for Use as Ligands in Asymmetric Catalysis

✍ Scribed by Mino, Takashi; Tanaka, Youichi; Hattori, Youtaro; Yabusaki, Toshihiro; Saotome, Hiroaki; Sakamoto, Masami; Fujita, Tsutomu

Book ID
127326295
Publisher
American Chemical Society
Year
2006
Tongue
English
Weight
180 KB
Volume
71
Category
Article
ISSN
0022-3263

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ChemInform Abstract: Kinetic Resolution
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A C(aryl)N(amine) bond atropisomeric am
A C(aryl)N(amine) bond atropisomeric aminophosphine: preparation and use as a ligand in a catalytic asymmetric allylic alkylation
✍ Takashi Mino; Youichi Tanaka; Toshihiro Yabusaki; Daisuke Okumura; Masami Sakamo 📂 Article 📅 2003 🏛 Elsevier Science 🌐 English ⚖ 193 KB

The existence of 3 as a pair of stable atropisomers has been demonstrated analytically through chiral phase LC-CD investigations. Resolution of 3d was achieved by preparative chiral HPLC. Finally, the ability of the first C(aryl) N(amine) axially chiral phosphine ligand 3d is demonstrated in a catal