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Synthesis and odour characteristics of racemic and optically active oxy-derivatives of gem-dimethylcyclohexene

✍ Scribed by Katarzyna Wińska; Józef Kula; Czesław Wawrzeńczyk

Publisher
John Wiley and Sons
Year
2011
Tongue
English
Weight
684 KB
Volume
26
Category
Article
ISSN
0882-5734

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## ABSTRACT Enantioselective syntheses of two stereoisomers of 3‐hydroxy‐4‐phenyl‐2‐butanone were investigated via Shi's asymmetric epoxidation or Sharpless asymmetric dihydroxylation of silyl enol ether. (__R__)‐3‐Hydroxy‐4‐phenyl‐2‐butanone was obtained in 73% enantiomeric excess (__ee__) by Shi'