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Synthesis and microbiological hydroxylation of 16α,17α-dihydroxy-substituted 20-OXO-5α-pregnanes

✍ Scribed by M. L. Gerasimova; T. I. Gusarova; V. M. Ryzhkova; T. M. Bykova; L. M. Alekseeva


Book ID
112400482
Publisher
Springer
Year
1989
Tongue
English
Weight
516 KB
Volume
23
Category
Article
ISSN
0091-150X

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Synthesis of 5α-pregnane-3β,20α-diol and
✍ T. A. Baillie; J. E. Herz; J. Sjövall 📂 Article 📅 1974 🏛 John Wiley and Sons 🌐 French ⚖ 241 KB 👁 1 views

## Abstract A convenient synthesis of 5α‐[20β‐^2^H]pregnane‐3α,20α‐diol and 5α‐[20β‐^2^H]pregnane‐3β,20α‐diol from 3β‐hydroxy‐5α‐pregn‐16‐en‐20‐one is described. The reaction products are characterized by combined gas chromatography‐mass spectrometry.