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Synthesis and mesomorphic properties of 1-(4′-ethyl biphenylyl) 2-(4-alkoxy-2,3,5,6-tetrafluorophenyl) acetylenes

✍ Scribed by Xu Yue-Lian; Yin Hui-Yong; Wang Wei-Li; Chen Qi; Wen Jian-Xun

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
348 KB
Volume
14
Category
Article
ISSN
0256-7660

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## Abstract [4″‐^3^H]‐2‐(1‐[2″,6″‐Dichlorophenoxy]‐ethyl‐Δ^2^‐imidazoline) was prepared from [4‐^3^H]‐2,6‐dichlorophenol in two different ways. By reaction of 2,6‐dichlorophenol with 2‐(α‐chloroethyl)‐Δ^2^‐imidazoline, the radiochemical yield, at a specific activity of 173.9 mCi/mmole, was 12.8 %.