## Abstract The ^17^O NMR chemical shifts of five enriched amino acids have been measured under strictly controlled conditions of concentration, ionic strength, pH and temperature. The Ξ±, Ξ² and Ξ±, Ξ³ carboxyl resonances of aspartic and glutamic acid, respectively, have been resolved. Line widths wer
β¦ LIBER β¦
Synthesis and magnetic resonance studies of some phosphinous acids, phosphorylacetic acids, and some of their coordination compounds
β Scribed by Samuel O. Grim; Larry C. Satek
- Book ID
- 115974579
- Publisher
- Elsevier Science
- Year
- 1977
- Weight
- 736 KB
- Volume
- 39
- Category
- Article
- ISSN
- 0022-1902
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## Abstract ^17^O chemical shifts of four amino acids at natural abundance have been obtained. Sensitivity was enhanced by accumulating a large number of scans or employing high concentrations at elevated temperature. Routine memory overflow was avoided by using a combination of solvent suppression
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