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17O nuclear magnetic resonance studies of some amino acids at natural abundance

✍ Scribed by B. Valentine; T. St Amour; R. Walter; D. Fiat

Publisher: John Wiley and Sons
Year: 1980
Tongue: English
Weight: 120 KB
Volume: 13
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1270130318

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✦ Synopsis

Abstract

^17^O chemical shifts of four amino acids at natural abundance have been obtained. Sensitivity was enhanced by accumulating a large number of scans or employing high concentrations at elevated temperature. Routine memory overflow was avoided by using a combination of solvent suppression and phase alternating pulse sequences.

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