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Synthesis and identification of 4-methyl-N-(4H-1,2,4-triazol-4-yl)-2-benzothiazolamine, an impurity in the synthesis of tricyclazole

โœ Scribed by Barry A. Dreikorn; Paul Unger


Book ID
112129444
Publisher
Journal of Heterocyclic Chemistry
Year
2009
Tongue
English
Weight
211 KB
Volume
26
Category
Article
ISSN
0022-152X

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A series of triorganotin (4H-1,2,4triazol-4-yl)benzoates have been synthesized by the reaction of 4-( 4H-1,2,4-triazol-4-yl)benzoic acid and 3-(4H-1,2,4-triazol-4-yl)benzoic acid with (R 3 Sn) 2 O (R = Et, n-Bu and Ph) or R 3 SnOH (R = p-tolyl and cyclohexyl). The molecular structure of tri( p-tolyl