Synthesis and Crystal Structure of Octahydro-5H,12H-4,11-methano-1H,7H-bis[1,2,5]oxadiazolo[3,4-d:3′,4′-j][1,7,3,9]dioxadiazacyclododecine
✍ Scribed by Rodney L. Willer; Robson F. Storey; William L. Jarrett; Damon Parrish
- Book ID
- 112131802
- Publisher
- Journal of Heterocyclic Chemistry
- Year
- 2012
- Tongue
- English
- Weight
- 130 KB
- Volume
- 49
- Category
- Article
- ISSN
- 0022-152X
- DOI
- 10.1002/jhet.926
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📜 SIMILAR VOLUMES
The asymmetric unit of the title compound, C 19 H 16 FN 5 O 4 , contains two independent molecules. The dihedral angles between the main planes and the fluorophenyl rings in the two molecules are 83.24 (5) and 71.76 (4) . Weakstacking interactions may be effective in the stabilization of the crystal
## Abstract H~10~TTPR was prepared starting from terephthalaldehyde and characterized. Crystal structure of H~10~TTPR and an intermediate compound 11 were determined by X‐ray diffraction analysis. A quasi‐reversible redox wave at 1.15 V (vs. SCE) was observed for H~10~TTPR, indicating that it is a