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Synthesis and crystal structure of new alkali metal hydrogen tellurates

✍ Scribed by A. V. Churakov; E. A. Ustinova; P. V. Prikhodchenko; T. A. Tripol’skaya; J. A. K. Howard


Book ID
110180754
Publisher
SP MAIK Nauka/Interperiodica
Year
2007
Tongue
English
Weight
305 KB
Volume
52
Category
Article
ISSN
0036-0236

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✍ Sabine Herzog; Christian Näther; Peter Dürichen; Wolfgang Bensch 📂 Article 📅 1998 🏛 John Wiley and Sons 🌐 German ⚖ 93 KB 👁 2 views

Needle-shaped, moisture sensitive, yellow crystals of Na 3 TaS 4 were obtained by the reaction of Na 2 S 3 , Ta, and S at 450 °C. The structure was determined by single crystal X-ray diffraction and refined to R1 and wR2 values of 0.0172 and 0.0381, respectively. Na 3 TaS 4 crystallizes with 32 form