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Synthesis and crystal structure of [Co(mpt)2{P(OCH3)3}2]BF4 (Hmpt = 2-mercaptothiazoline)

✍ Scribed by Ye-Xiang Tong; Bei-Sheng Kang; Cheng-Yong Su; Xiao-Lan Yu; Xiao-Ming Chen

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
327 KB
Volume
17
Category
Article
ISSN
0256-7660

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## Abstract The monosubstituted [Ir~4~(CO)~11~L] clusters (L = P(OPh)~3~, 1; L = P(OMe)~3~, 2; L = P(OCH~2~)~3~CEt, 3) were obtained in good yields by the reaction of [Ir~4~(CO)~11~I]^βˆ’^ with the corresponding phosphite. In the solid state, cluster 3 has a __C__~__s__~ geometry with all terminal li