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Synthesis and Crystal Structure of an Unprecedented Supramolecular Complex [Co(µ2-ClO4)2(H2O)2]·2MA

✍ Scribed by Jing XU; Zhengshuai BAI; Weiyin SUN

Publisher
John Wiley and Sons
Year
2009
Tongue
English
Weight
158 KB
Volume
27
Category
Article
ISSN
0256-7660

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Perchlorato Complexes of Rare-Earth Elements: Syntheses and Crystal Structures of Lu(ClO4)3 · 3 H2O, Er(ClO4)3 · H2O, and Sc(OH)(ClO4)2 · H2O
✍ Mathias S. Wickleder 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 German ⚖ 181 KB 👁 2 views

Single crystals of Lu(ClO 4 ) 3 ´3 H 2 O were obtained by slow dehydration of Lu(ClO 4 ) 3 ´6 H 2 O at 140 °C under flowing argon. The compound crystallizes in the triclinic crystal system (P1, Z = 2, a = 750.3(1), b = 838.4(1), c = 1054.6(2) pm, a = 79.77(2)°, b = 79.18(2), c = 63.83(2), R all = 0.