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Synthesis and crystal structure of an ionic cluster {[Mo3(μ3-O)(μ-S)3(dtp)3(py)3][CdI(dtp)2]}

✍ Scribed by Shao-Fang Lu; Jian-Quan Huang; Xiao-Ying Huang; Qiang-Jin Wu

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
435 KB
Volume
15
Category
Article
ISSN
0256-7660

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A new cluster of formula {[Mo 3 (μ 3 -S)(μ-S)(μ-S 2 ) 2 (dtp) 3 (μ-OAc)][Mo 3 NiS 4 (dtp) 3 (μ-OAc)(CH 3 CN)]} (1; dtp = diethyl dithiophosphate; OAc = acetate) comprising the novel C s -symmetrized Mo 3 (μ 3 -S)(μ-S)(μ-S 2 ) 2 structural type covalently attached to a cubane-type Mo 3 NiS 4 core has