✦ LIBER ✦

Synthesis and Crystal Structure of a Novel Zincophosphite Containing Two-dimensional Inorganic-organic Network

✍ Scribed by Ya-Li Yang; Niu Li; Shou-He Xiang

Publisher: John Wiley and Sons
Year: 2010
Tongue: English
Weight: 270 KB
Volume: 22
Category: Article
ISSN: 0256-7660
DOI: 10.1002/cjoc.20040220406

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✦ Synopsis

A novel 1.6-hexamethylenedia-~~phosphite has been synthesized hydrothemally. Its single-crystal smcnue rebemat has shown the zincophosphitc with the composition NH; (CH& NH; [Zn(HPC&)z12-, M,= 343.55. It crystallizes in monoclinic, space group CUc (NO. 15). a=2.2391 NU. l~0.8695 nm, c=0.7919 nm, /3= 101.062(6)0, V= 1.513 tun3, 0,=1.508 kg/m3, 2=4, F(000)=712, p= 1.849 mm-', RI=0.0416. wR2=O.1023. This phase exhibits infinite inorganic chains of vertex-linkcd ZnO4 and HPO,. Via the electrostatic attraction, 1.6-hexmethylenediamine cations and inorganic chairis construct a novel interesting two-dimensional inorganic-organic network.

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