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Synthesis and crystal structure of 2-benzoyl-4-methyl phenyl benzoate

✍ Scribed by M. Mahendra; B. H. Doreswamy; M. A. Sridhar; J. Shashidhara Prasad; S. A. Khanum; S. Shashikanth; T. D. Venu


Publisher
Springer
Year
2005
Tongue
English
Weight
105 KB
Volume
35
Category
Article
ISSN
1572-8854

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4-Amino[7-14C]benzoic acid (3) is prepared by carbonation of tHe lithium salt of N,N-bis(trimethylsilyl)aniline. The methyl ester (4) of 3 is generated with trimethylsilyldiazomethane, and 4 is coupled with 2,5-dihydroxybenzaldehyde to yield methyl 4-(2,5-dihydroxybenzylimino)[7-14C]benzoate (5). 5