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Synthesis and Crystal Structure Determination of 3,4-Dimethoxybenzyl 2,3,4-Trimethoxyphenyl Ketone

✍ Scribed by M. I. Arriortua; J. Via; M. K. Urtiaga; E. Domínguez; A. Igartua; N. Sotomayor

Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
269 KB
Volume
100
Category
Article
ISSN
0037-9646

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The compounds [TeI 3 ][MI 4 ] (M = Ga, In) were obtained as air sensitive black crystals by the reactions of Te, I 2 and Ga or In in vacuum sealed ampoules. The gallium compound crystallizes in the structural type of [SCl 3 ][AlCl 4 ]: monoclinic system, space group Pc (No. 7), a = 7.211(11), b = 7.