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Synthesis and configuration of diastereomeric 2-substituted 5-oxoquinuclidines

✍ Scribed by L. I. Mastafanova; K. F. Turchin; L. M. Alekseeva; Yu. N. Sheinker; L. N. Yakhontov

Book ID
112489266
Publisher
Springer US
Year
1971
Tongue
English
Weight
643 KB
Volume
7
Category
Article
ISSN
0009-3122

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The first studies toward the solid-phase synthesis of 1,4,5-substituted-2-oxopiperazines are reported. The synthetic strategy is based on reductive alkylation of resin-bound amino acids using N-protected a-amino aldehydes (with concomitant epimerization), followed by acylation with a-chloroacetyl ch