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Stereochemistry of cyclic compounds—I : Synthesis and configurational assignment of diastereomeric 2,4-dioxaspiro[5.5]undec-8-enes

✍ Scribed by Klaus Bruns; Jens Conrad; Alois Steigel


Publisher
Elsevier Science
Year
1979
Tongue
French
Weight
628 KB
Volume
35
Category
Article
ISSN
0040-4020

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has been hydrothermally synthesized and structurally characterized by single-crystal X-ray diffraction. Black crystals crystallize in the tetragonal system, space group I4/m, a = b = 14.019(2) A ˚, c = 20.341(4) A ˚, V =3997.9(11) A ˚3, Z = 2, k(MoKa) = 0.71073 A ˚(R(F) = 0.0443 for 1819 reflections