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Synthesis and complexation properties of a new macrocyclic polyaza polyphosphinate ligand, DOTEP (1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrakis(methyleneethylphosphinate))

✍ Scribed by Lazar, Istvan.; Sherry, A. Dean.; Ramasamy, Ravichandran.; Brucher, Erno.; Kiraly, Robert.

Book ID: 126091751
Publisher: American Chemical Society
Year: 1991
Tongue: English
Weight: 555 KB
Volume: 30
Category: Article
ISSN: 0020-1669
DOI: 10.1021/ic00026a030

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Aktnrlz The reaction of 1.4,7,10-tctraazd~yoModccanc with p-toluenenrlfonyl chloride in pyridinc or with diethyl phowhite and Ccl, in a water/CH&l, mixture yielda sclaotivcly the 1.7diprotcctcd regiokacr. The 1.7-dipmtected tfAraax.9 cycles are interesting Starting mstcrinls. for instana for Ihe pr