Synthesis and Characterization of the cis- and trans-Trimethylsilylcyclohexanols 1
β Scribed by Fessenden, Ralph J.; Seeler, Keith; Dagani, Michael
- Book ID
- 126988307
- Publisher
- American Chemical Society
- Year
- 1966
- Tongue
- English
- Weight
- 708 KB
- Volume
- 31
- Category
- Article
- ISSN
- 0022-3263
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## Abstract __Trans__β4βd~β1~βtetranydronaphthalenβ1βol (__trans__β4βd~β1~β1β tetralol) was synthesized from 1,4βepoxyβ1,2,3,4β tetrahydronaphthalene using lithium triβ__tert__βbutoxyaluminodeuteride. __Cis__β4βd~β1~β1βtetralol was made by epimerizing the __trans__β compound. Both compounds were ch
A preparative route to cis-and trans-1,2-dibromocyclopropane ' Trans-& b.p. (120Β°C/300 mbar) and H NMR spectrum were In agreement with the literature 2 ; w m.p. 8OC; b.p. 120Β°C/100 mbar; 'H NMR spectrum (CDC13, 250 Mhz): 6 = 3.10 ppm (dd,