✦ LIBER ✦

Synthesis and Characterization of Ternary CuInS2 Nanorods via a Hydrothermal Route

✍ Scribed by Jianping Xiao; Yi Xie; Rui Tang; Yitai Qian

Publisher: Elsevier Science
Year: 2001
Tongue: English
Weight: 304 KB
Volume: 161
Category: Article
ISSN: 0022-4596
DOI: 10.1006/jssc.2001.9247

No coin nor oath required. For personal study only.

✦ Synopsis

Well-de5ned ternary CuInS 2 nanorods 20+25 nm in diameter and 400+450 nm in length were synthesized by the reaction of CuCl 2 , In, CS 2 , and NaOH at temperature as low as 1803C for 15 h when water was used as the solvent. The products were characterized by X-ray di4raction, transmission electron microscopy, selected area electron di4raction, X-ray photoelectron spectroscopy, and UV+vis absorption spectroscopy techniques. Experimental results indicate that reaction temperature is an important factor in this approach and liquid indium plays an important role in the formation of CuInS 2 nanorods. Finally, a solution+liquid+solid mechanism was proposed for the nanorod growth.

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