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Synthesis and characterization of bis(O,O′-diisopropylmonothiophosphato)nickel(II) adducts and molecular structures of bis(pyridine)bis(O,O′-diisopropylmonothiophosphato)nickel(II) complex

✍ Scribed by Subhash C. Bajia; Anurag Mishra; Ray J. Butcher

Publisher: Springer
Year: 2011
Tongue: English
Weight: 259 KB
Volume: 36
Category: Article
ISSN: 0340-4285
DOI: 10.1007/s11243-011-9474-2

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We have now been able to show that a nucleophilic addition takes place on reaction of triphenylstannyllithium with carbon disulfide. The initial product (1) can be trapped by alkylation with methyl or ethyl iodide in tetrahydrofuran (THE'). ## 20 "c After separation by column chromatography, the p