Synthesis and Characterisation of Alkali
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PrimoΕΎ BenkiΔ; H. Donald Brooke Jenkins; Maja Ponikvar; Zoran Mazej
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Article
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2006
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John Wiley and Sons
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English
β 211 KB
## Abstract Reactions of AF (A = K, Rb, Tl) with excess liquid SbF~5~ in anhydrous HF (or SO~2~) at room temperature give products having the composition ASb~2~F~11~. The reaction between CsF and a small excess of SbF~5~ in anhydrous HF (0.76 mmol of CsF + 4.19 mmol of SbF~5~ in 4 mL of aHF) yields