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Synthesis and characterization of a series of trans-[Mo(CO)5(R2PNHCH2CH2NCHC6H4-o-O)]2M (R2  Ph2, OCH2CMe2CH2O; M  Co, Ni, Cu) complexes and the crystal structure of trans-[Mo(CO)5(Ph2PNHCH2-CH2-NCHC6H4-o-O)]2Ni · 2Et2O

✍ Scribed by Gary M. Gray; Naoto Takada; Alan L. Zell; Howard Einspahr

Book ID
107811207
Publisher
Elsevier Science
Year
1988
Tongue
English
Weight
995 KB
Volume
342
Category
Article
ISSN
0022-328X

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Photolysis of the cis-Mo(CO) 4 {Ph 2 P(CH 2 CH 2 O) n CH 2 CH 2 PPh 2 -P,P%}, (1, n= 3; 2, n= 4; 3, n= 5) metallacrown ethers in tetrahydrofuran under nitrogen gives moderate yields of the corresponding trans-Mo(CO) 4 {Ph 2 P(CH 2 CH 2 O) n CH 2 CH 2 PPh 2 -P,P%} (4, n =3; 5, n= 4; 6, n= 5) metallac