## Abstract **Summary:** A new calix[4]arene‐based periodic mesoporous organosilica has been synthesized using tetraethoxysilane (TEOS) and a calix[4]arene‐based silane monomer as the precursors and cetyltrimethylammonium bromide (CTAB) surfactant as the structure‐directing template, and is shown t
Synthesis and Characterization of a Novel, Mesoporous Organosilica with Additional Cyclodextrin-Based Micropores
✍ Scribed by Chunqing Liu; Jinfeng Wang; James Economy
- Publisher
- John Wiley and Sons
- Year
- 2004
- Tongue
- English
- Weight
- 131 KB
- Volume
- 25
- Category
- Article
- ISSN
- 1022-1336
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
Summary: A novel mesoporous organosilica with additional cyclodextrin‐based micropores has been synthesized from tetraethoxysilane (TEOS) and cyclodextrin‐based silane monomer precursors and triblock PEO‐PPO‐PEO (poly(ethylene oxide)‐poly(propylene oxide)‐ poly(ethylene oxide)) copolymer P123 as the structure‐directing template with the aid of sodium chloride and the supramolecular assembly of cyclodextrins with P123.
The synthesis of CD‐Si‐2%.
imageThe synthesis of CD‐Si‐2%.
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## Abstract Two novel monovinyl __β__‐cyclodextrin (__β__‐CD) monomers are synthesized. Their chemical compositions are characterized by means of element analysis, NMR and FT‐IR spectroscopy. The results show that the synthesis techniques used are convenient and efficient. Using __N__‐isopropylacry