Synthesis and characterization of 4-aryl-5-(1-aryl-2-methyl-2-nitropropyl)-1,2,3-selenadiazoles

✍ Scribed by Sivaperuman Saravanan; Arumugam Nithya; Shanmugam Muthusubramanian

• Publisher: Journal of Heterocyclic Chemistry
• Year: 2006
• Tongue: English
• Weight: 294 KB
• Volume: 43
• Category: Article
• ISSN: 0022-152X
• DOI: 10.1002/jhet.5570430122

✦ Synopsis

Abstract

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The synthesis of a new set of selenadiazoles, 4‐aryl‐5‐(1‐aryl‐2‐methyl‐2‐nitropropyl)‐1,2,3‐selenadiazoles (4) derived from 2‐[4‐methyl‐4‐nitro‐1,3‐diarylpentylidene]‐1‐hydrazinecarboxamide (3) has been reported. THF has been found to be the solvent of choice for this reaction. Structural features of 3 and 4 have been analyzed by NMR and X‐ray techniques.