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Synthesis and biological activity of 25,26,27-trisnor-vitamin D3 24-oic acid and its 1α-hydroxyl analog

✍ Scribed by Koizumi Naoyuki; Morisaki Masuo; Ikekawa Nobuo; Tanaka Yoko; Hector F. Deluca

Book ID
116001654
Publisher
Elsevier Science
Year
1979
Tongue
English
Weight
622 KB
Volume
10
Category
Article
ISSN
0022-4731

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✍ Rafal R. Sicinski; Yoko Tanaka; Mary Phelps; Heinrich K. Schnoes; Hector F. DeLu 📂 Article 📅 1987 🏛 Elsevier Science 🌐 English ⚖ 573 KB

Synthesis of a C-24-epimeric mixture of 25-hydroxy-[26,27-3H]vitamin D2 and a C-24-epimeric mixture of 1,25-dihydroxy-[26,27-'HIvitamin D2 by the Grignard reaction of the corresponding 25-keto-27-nor-vitamin D2 and lo-acetoxy-25keto-27-nor-vitamin D3 with tritiated methyl magnesium bromide is descri