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Syntheses with stable isotopes: 4-Ethylsulfonyl-l-naphthalenesulfonamide- 15N

✍ Scribed by Thomas W. Whaley; Guido H. Daub

Publisher
John Wiley and Sons
Year
1977
Tongue
French
Weight
211 KB
Volume
13
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

The title compound was prepared from 4‐ethylthio‐1‐naphalenesulfonyl chloride in a two‐step synthesis with an overall yield of 56%. An alternative one‐step synthesis from 4‐ethylsulfonyl‐1‐naphthalenesulfonyl chloride was found to be unsuitable for nitrogen labeling.

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