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Syntheses of the opioid substructures 1,2,3,4,5,6-hexahydro-2,6-methano-3-benzazocine and 2,3,4,5-tetrahydro-1,5-methano-1H-2-benzazepine

✍ Scribed by Jotham W. Coe; Paige R. Brooks; Michael G. Vetelino; Crystal G. Bashore; Krista Bianco; Andrew C. Flick

Publisher
Elsevier Science
Year
2011
Tongue
French
Weight
320 KB
Volume
52
Category
Article
ISSN
0040-4039

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2-(2,2-Dimethoxyethyl)-3-oxo-1,2,3,4,5,6
2-(2,2-Dimethoxyethyl)-3-oxo-1,2,3,4,5,6-hexahydro-1,5-methano-7H-azocino[4,3-b]indole
✍ HΓΆkelek, Tuncer ;Şahin, Ertan ;Uludağ, Nesimi ;Erdoğan, Ümit Işık πŸ“‚ Article πŸ“… 2007 πŸ› International Union of Crystallography 🌐 English βš– 894 KB

The title compound, C 18 H 22 N 2 O 3 , consists of a tetracyclic ring system containing an azocino skeleton with a dimethoxyethyl group as a substituent. The benzene and five-membered rings are nearly coplanar, with a dihedral angle of 1.26 (8) . In the crystal structure, intermolecular N-HÁ Á ÁO h

A novel entry into 1,2,3,4,5,6-hexahydro
A novel entry into 1,2,3,4,5,6-hexahydro-3-benzazocine-4,6-dione and 2-substituted-2,5,6,7-tetrahydro-4-benzazonine-1,3-(4H)-dione
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Z-Substituted-1,2,3,4,5,6-hexahydro-3-bemwxine-4, 6diones(la-d) and 2-methoxy-2,5,6,7-tetrahydro+ benxamnine-1,3dione 8 were synthesii thro@ an oxklative ring expansion reaction of 6-methylthio-7-substiituted-benzo(a] octem (2a-d ) and 7-methylthio%-methoxy-benzo[a]nonem 7 with sodium periodate in i