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Syntheses of seven-membered cyclic azo compounds

✍ Scribed by Overberger, C. G.; Merkel, Timothy F.

Book ID: 127201368
Publisher: American Chemical Society
Year: 1981
Tongue: English
Weight: 762 KB
Volume: 46
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00315a041

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We wish to report the preparations of the first medium-sized cyclic aso compounds possessing trans-aso linkages, namely, trans-1,2-diaza-1-cyclooctene (A), trans-3,8-dimethyl-trans-1,2-diaza-1-cyclooctene (11, trans-l,Z-diaza-lcyclononene (2) and trans-1,2-diasa-1-cyclodecene (4). Irradiation of o&-