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Syntheses of Lignin-Derived Thioacidolysis Monomers and Their Uses as Quantitation Standards

โœ Scribed by Yue, Fengxia; Lu, Fachuang; Sun, Run-Cang; Ralph, John


Book ID
115525320
Publisher
American Chemical Society
Year
2012
Tongue
English
Weight
332 KB
Volume
60
Category
Article
ISSN
0021-8561

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Syntheses of deuterated leu-enkephalins
โœ Dr. E. Benfenati; G. Icardi; S. Chen; R. Fanelli ๐Ÿ“‚ Article ๐Ÿ“… 1990 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 348 KB

## Abstract We have developed a synthetic method for the preparation of diโ€ and pentadeuterated leuโ€enkephalin (LE), Tyrโ€Glyโ€Glyโ€Pheโ€Leu, by protonโ€deuterium exchange using CF~3~COO^2^H. Four to six deuterium atoms are introduced using a reaction temperature of 120ยฐC and if 5% of ^2^H~2~O is added