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Syntheses of cis- and trans-tetraamminedichlororuthenium(III) chloride

✍ Scribed by Susan E. Boggs; Richard E. Clarke; Peter C. Ford

Book ID
103111510
Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
164 KB
Volume
247
Category
Article
ISSN
0020-1693

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Total syntheses of (±)-cis- and trans-11
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✍ Kalle Rönkkö; Mathias Berner; Reija Jokela; Arto Tolvanen 📂 Article 📅 2000 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 302 KB

## Abstract The total syntheses of 11‐methoxydeethyleburnamonines (**4**) and (**13**) were carried out with use of 6‐methoxytryptophyl bromide (**5**) as starting material. Compound **5** was converted in three steps to __trans__‐ester **8**. Acid‐catalysed epimerization of **8**, lithium aluminum