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Syntheses of 1,4-butanediamine-1,1,4,4-d4, 1,4-butanediamine-2,2,3,3-d4, and their respective bis(ammonium nitrate) salts

✍ Scribed by Alan P. Marchand; N. Satyanarayana; Robert L. McKenney Jr.; Stephen R. Struck

Publisher: John Wiley and Sons
Year: 1988
Tongue: French
Weight: 258 KB
Volume: 25
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580250908

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✦ Synopsis

Syntheses o f t h e t i t l e compounds from d i e t h y l succinate and from dimethyl acetylenedicarboxylate i n 16% and 18% o v e r a l l y i e l d , respectively, are described; a procedure f o r converting these s p e c i f i c a l l y deuterated diamines i n t o the corresponding bis(ammonium n i t r a t e ) s a l t s i n 62% and 66% y i e l d , r e s p e c t i v e l y , i s presented.

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