Syntheses Based on 2-Methyl-5-nitrogramine. Preparation of 2-Methyl-5-nitroindole-3-acetic Acid
โ Scribed by Noland, Wayland E.; Rush, Kent R.
- Book ID
- 127070480
- Publisher
- American Chemical Society
- Year
- 1963
- Tongue
- English
- Weight
- 291 KB
- Volume
- 28
- Category
- Article
- ISSN
- 0022-3263
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๐ SIMILAR VOLUMES
A synthesis of 3-cyano-4-methyl-5 ( 14 C)-methyl-2-(5-14C)pyrrolyloxamic acid is described. The compound, having specific activity of 66.7 pCi/mmole, was obtained in 19.68% overall yield from uniformly labelled 14C-l-alanine. 14 14 Key Words: 3-Cyano-4-methyl-5( C)-methyl-2-(5-C)pyrrolyloxamic acid,
All interatomic distances in the title compound, C~5~H~7~N~3~O~2~S, are normal. The 1,2,4-triazoline ring is planar and it is inclined at 78.61โ (7)ยฐ to the planar acetic acid group. The molecules of the title compound are connected __via__ OโH...N hydrogen bonds into zigzag chains along the [101] di