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Syntheses and structural studies of heterobimetallic thiocarboxylate complexes containing zinc and copper

✍ Scribed by Singh, Suryabhan; Chaturvedi, Jyotsna; Aditya, A.S.; Rajasekhar Reddy, N.; Bhattacharya, Subrato

Book ID: 120073090
Publisher: Elsevier Science
Year: 2013
Tongue: English
Weight: 745 KB
Volume: 396
Category: Article
ISSN: 0020-1693
DOI: 10.1016/j.ica.2012.11.022

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The reaction of the lithium β-diketoiminate complex (dipp with ZnCl 2 yielded the corresponding (dipp)NacNacZnCl ( 1) and (dipp)NacNacZn(µ-Cl) 2 Li(OEt 2 ) 2 (1a). Treatment of 1 with LiCϵCPh and NaBH 4 in diethyl ether gave (dipp)Nac-NacZnCϵCPh ( 2) and (dipp)NacNacZn(µ-H) 2 BH 2 (3). The core ele