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Synthese von 2-substituiertem 2,3-Dihydro-1H-dibenzo [b, f]pyrazolo [1,2-d] [1,4,5] thiadiazepin-9-dioxid-1,3-dion. Über Pyrazole, 2. Mitteilung

✍ Scribed by K. Michel; M. Matter


Publisher
John Wiley and Sons
Year
1961
Tongue
German
Weight
346 KB
Volume
44
Category
Article
ISSN
0018-019X

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✦ Synopsis


Abstract

Es wird die Herstellung des bisher nur unrein bekannten 2,2′‐Di‐hydroxyl‐amino‐diphenylsulfons (IV) als reine, haltbare Verbindung beschrieben. Daraus werden 5,6‐Dihydro‐dibenzo[1, 4,5]thiadiazepin‐ll‐dioxid (VI), dessen N, N′‐Di‐acetylderivat VIII sowie die 2‐Butyl‐Hexyl‐ und ‐Tetrahydrofurfuryl‐2,3‐dihydro‐1__H__‐dibenzo[b, f]pyrazolo[1, 2‐d] [1,4,5] thiadiazepin‐9‐dioxid‐1,3‐dione (II) synthetisiert.


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