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Synthese und Molekülstruktur chiraler Bis(1,3,2-dioxaphospholane)

✍ Scribed by P. Krüger; B. Weberndörfer; H. Werner

Publisher
John Wiley and Sons
Year
2000
Tongue
German
Weight
189 KB
Volume
626
Category
Article
ISSN
0372-7874

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✍ Viktor P. Balema; Steffen Blaurock; Evamarie Hey-Hawkins 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 German ⚖ 91 KB

Rac-1,2-bis(chlorophenylphosphino)-1,2-dicarbacloso-dodecaborane(12) (1) reacts with [Mo(CO) 4 (NBD)] (NBD = norbornadiene) after several hours at 50±55 °C to yield cis-rac-[Mo(CO) 4 {1,2-(PPhCl) 2 C 2 B 10 H 10 }] (2). 2 was characterised spectroscopically ( 1 H, 13 C, 11 B and 31 P NMR) and by cry