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Ein 1,2-Phenylen-verbrücktes Porphyrindimer - Synthese, Eigenschaften und Molekülstruktur

✍ Scribed by Prof. Atsuhiro Osuka; Satoshi Nakajima; Toshi Nagata; Prof. Kazuhiro Maruyama; Prof. Koshiro Toriumi

Publisher
John Wiley and Sons
Year
1991
Tongue
English
Weight
227 KB
Volume
103
Category
Article
ISSN
0044-8249

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Rac-1,2-bis(chlorophenylphosphino)-1,2-dicarbacloso-dodecaborane(12) (1) reacts with [Mo(CO) 4 (NBD)] (NBD = norbornadiene) after several hours at 50±55 °C to yield cis-rac-[Mo(CO) 4 {1,2-(PPhCl) 2 C 2 B 10 H 10 }] (2). 2 was characterised spectroscopically ( 1 H, 13 C, 11 B and 31 P NMR) and by cry