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Synthese, Eigenschaften und Struktur von [Li(OC4H8)4][((CH3)3Si)3C–InBr3]

✍ Scribed by A. Walz; K. W. Klinkhammer; J. Weidlein

Publisher
John Wiley and Sons
Year
1998
Tongue
German
Weight
84 KB
Volume
624
Category
Article
ISSN
0372-7874

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✦ Synopsis

The reaction of InBr 3 with LiR* ´(THF) n (R* = ±C(SiMe 3 ) 3 , THF = OC 4 H 8 ) in a 1 : 1 molar ratio forms [Li(THF) 4 ][R*InBr 3 ] in good yield. The properties and some spectroscopic data ( 1 H, 13 C, 29 Si, 7 Li±NMR, IR and Raman) of this trisyl-tribromoindate are given and the crystal structure has been determined.

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