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Synthese des tritiummarkierten eberpheromons [5α, 6α-3H]-5α-androst-16-en-3-on

✍ Scribed by H. Wagner; J. Römer


Publisher
John Wiley and Sons
Year
1978
Tongue
French
Weight
329 KB
Volume
14
Category
Article
ISSN
0022-2135

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✦ Synopsis


The synthesis of [5α, 6α‐^3^H]‐5α‐androst‐16‐en‐3‐one, starting with the catalytic tritiation of 3β‐acetoxy‐androst‐5‐en‐17‐one, is described. The so‐called “boar taint ketone” was obtained with high specific activity (21 Ci/mmol) and radiochemical purity better than 98 %.


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